Fundamentals of Analytical Chemistry 10th Edition by Douglas A. Skoog, ISBN-13: 978-0357450390

Description

Fundamentals of Analytical Chemistry 10th Edition by Douglas A. Skoog, ISBN-13: 978-0357450390

[PDF eBook eTextbook]

• Publisher: ‎ Cengage Learning; 10th edition (August 4, 2021)
• Language: ‎ English
• 1072 pages
• ISBN-10: ‎ 0357450396
• ISBN-13: ‎ 978-0357450390

Discover the principles and practices behind analytical chemistry as you study its applications in medicine, industry and the sciences with Skoog/West/Holler/Crouch’s FUNDAMENTALS OF ANALYTICAL CHEMISTRY, 10th Edition. This award-winning author team presents the latest developments in analytical chemistry today using a reader-friendly yet systematic and thorough approach. Each chapter begins with a compelling story and stunning visuals. Dynamic photos from renowned chemistry photographer Charlie Winters capture attention while reinforcing key principles. New features highlight chemistry-related careers. You also learn how to use Excel 2019 as a problem-solving tool in analytical chemistry with new exercises, examples and a no-cost supplement by the text authors. OWLv2 online homework tool is also available to help you master the principles of analytical chemistry today.

Table of Contents:

Contents in Brief

Contents

Preface

Chapter 1: The Nature of Analytical Chemistry

1A The Role of Analytical Chemistry

1B Quantitative Analytical Methods

1C A Typical Quantitative Analysis

1D An Integral Role for Chemical Analysis: Feedback Control Systems

Part I: Quality of Analytical Measurements

Chapter 2: Calculations Used in Analytical Chemistry

2A Some Important Units of Measurement

2B Solutions and Their Concentrations

2C Chemical Stoichiometry

2D Calculations Using Microsoft Excel

Chapter 3: Precision and Accuracy of Chemical Analyses

3A Some Important Terms

3B Systematic Errors

Chapter 4: Random Errors in Chemical Analysis

4A The Nature of Random Errors

4B Statistical Treatment of Random Errors

4C Standard Deviation of Calculated Results

4D Reporting Computed Data

Chapter 5: Statistical Data Treatment and Evaluation

5A Confidence Intervals

5B Statistical Aids to Hypothesis Testing

5C Analysis of Variance

5D Detection of Gross Errors

Chapter 6: Sampling, Standardization, and Calibration

6A Analytical Samples and Methods

6B Sampling

6C Automated Sample Handling

6D Standardization and Calibration

6E Figures of Merit for Analytical Methods

Part II: Chemical Equilibria

Chapter 7: Aqueous Solutions and Chemical Equilibria

7A The Chemical Composition of Aqueous Solutions

7B Chemical Equilibrium

7C Buffer Solutions

Chapter 8: Effect of Electrolytes on Chemical Equilibria

8A The Effect of Electrolytes on Chemical Equilibria

8B Activity Coefficients

Chapter 9: Solving Equilibrium Problems for Complex Systems

9A Solving Multiple-Equilibrium Problems Using a Systematic Method

9B Calculating Solubilities by the Systematic Method

9C Separation of Ions by Control of the Concentration of the Precipitating Agent

Part III: Classical Methods of Analysis

Chapter 10: Gravimetric Methods of Analysis

10A Precipitation Gravimetry

10B Calculation of Results from Gravimetric Data

10C Applications of Gravimetric Methods

Chapter 11: Titrations in Analytical Chemistry

11A Some Terms Used in Volumetric Titrations

11B Standard Solutions

11C Volumetric Calculations

11D Gravimetric Titrations

11E Titration Curves

Chapter 12: Principles of Neutralization Titrations

12A Solutions and Indicators for Acid-Base Titrations

12B Titration of Strong Acids and Bases

12C Titration Curves for Weak Acids

12D Titration Curves for Weak Bases

12E The Composition of Solutions During Acid-Base Titrations

Chapter 13: Complex Acid-Base Systems

13A Mixtures of Strong and Weak Acids or Strong and Weak Bases

13B Polyfunctional Acids and Bases

13C Buffer Solutions Involving Polyprotic Acids

13D Calculation of the pH of Solutions of NaHA

13E Titration Curves for Polyfunctional Acids

13F Titration Curves for Polyfunctional Bases

13G Titration Curves for Amphiprotic Species

13H Composition of Polyprotic Acid Solutions as a Function of pH

Chapter 14: Applications of Neutralization Titrations

14A Reagents for Neutralization Titrations

14B Typical Applications of Neutralization Titrations

Chapter 15: Complexation and Precipitation Reactions and Titrations

15A The Formation of Complexes

15B Titrations with Inorganic Complexing Agents

15C Organic Complexing Agents

15D Aminocarboxylic Acid Titrations

Part IV: Electrochemical Methods

Chapter 16: Introduction to Electrochemistry

16A Characterizing Oxidation/Reduction Reactions

16B Electrochemical Cells

16C Electrode Potentials

Chapter 17: Applications of Standard Electrode Potentials

17A Calculating Potentials of Electrochemical Cells

17B Determining Standard Potentials Experimentally

17C Calculating Redox Equilibrium Constants

17D Constructing Redox Titration Curves

17E Oxidation/Reduction Indicators

17F Potentiometric End Points

Chapter 18: Applications of Oxidation/Reduction Titrations

18A Auxiliary Oxidizing and Reducing Reagents

18B Applying Standard Reducing Agents

18C Applying Standard Oxidizing Agents

Chapter 19: Potentiometry

19A General Principles

19B Reference Electrodes

19C Liquid Junction Potentials

19D Indicator Electrodes

19E Instruments for Measuring Cell Potential

19F Direct Potentiometry

19G Potentiometric Titrations

19H Potentiometric Determination of Equilibrium Constants

Chapter 20: Bulk Electrolysis: Electrogravimetry and Coulometry

20A The Effect of Current on Cell Potential

20B The Selectivity of Electrolytic Methods

20C Electrogravimetric Methods

20D Coulometric Methods

Chapter 21: Voltammetry

21A Excitation Signals in Voltammetry

21B Voltammetric Instrumentation

21C Hydrodynamic Voltammetry

21D Polarography

21E Cyclic Voltammetry

21F Pulse Voltammetry

21G Applications of Voltammetry

21H Stripping Methods

21I Voltammetry with Microelectrodes

Part V: Spectrochemical Analysis

Chapter 22: Introduction to Spectrochemical Methods

22A Properties of Electromagnetic Radiation

22B Interaction of Radiation and Matter

22C Absorption of Radiation

22D Emission of Electromagnetic Radiation

Chapter 23: Instruments for Optical Spectrometry

23A Instrument Components

23B Ultraviolet/Visible Photometers and Spectrophotometers

23C Infrared Spectrophotometers

Chapter 24: Molecular Absorption Spectrometry

24A Ultraviolet and Visible Molecular Absorption Spectroscopy

24B Automated Photometric and Spectrophotometric Methods

24C Infrared Absorption Spectroscopy

Chapter 25: Molecular Fluorescence Spectroscopy

25A Theory of Molecular Fluorescence

25B Effect of Concentration on Fluorescence Intensity

25C Fluorescence Instrumentation

25D Applications of Fluorescence Methods

25E Molecular Phosphorescence Spectroscopy

25F Chemiluminescence Methods

Chapter 26: Atomic Spectroscopy

26A Origins of Atomic Spectra

26B Production of Atoms and Ions

26C Atomic Emission Spectrometry

26D Atomic Absorption Spectrometry

26E Atomic Fluorescence Spectrometry

Chapter 27: Mass Spectrometry

27A Principles of Mass Spectrometry

27B Mass Spectrometers

27C Atomic Mass Spectrometry

27D Molecular Mass Spectrometry

Part VI: Kinetics and Separations

Chapter 28: Kinetic Methods of Analysis

28A Rates of Chemical Reactions

28B Determining Reaction Rates

28C Applications of Kinetic Methods

Chapter 29: Introduction to Analytical Separations

29A Separation by Precipitation

29B Separation of Species by Distillation

29C Separation by Extraction

29D Separating Ions by Ion Exchange

29E Chromatographic Separations

Chapter 30: Gas Chromatography

30A Instruments for Gas-Liquid Chromatography

30B Gas Chromatographic Columns and Stationary Phases

30C Applications of Gas-Liquid Chromatography

30D Gas-Solid Chromatography

Chapter 31: High-Performance Liquid Chromatography

31A Instrumentation

31B Partition Chromatography

31C Adsorption Chromatography

31D Ion Chromatography

31E Size-Exclusion Chromatography

31F Affinity Chromatography

31G Chiral Chromatography

31H Comparison of High-Performance Liquid Chromatography and Gas Chromatography

Chapter 32: Miscellaneous Separation Methods

32A Supercritical Fluid Separations

32B Planar Chromatography

32C Capillary Electrophoresis

32D Capillary Electrochromatography

32E Field-Flow Fractionation

Glossary

Appendix 1: The Literature of Analytical Chemistry

Appendix 2: Solubility Product Constants at 25 Degrees Celsius

Appendix 3: Acid Dissociation Constants at 25 Degrees Celsius

Appendix 4: Formation Constants at 25 Degrees Celsius

Appendix 5: Standard and Formal Electrode Potentials

Appendix 6: Use of Exponential Numbers and Logarithms

Appendix 7: Volumetric Calculations Using Normality and Equivalent Weight

Appendix 8: Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements

Appendix 9: Derivation of Error Propagation Equations

Answers to Selected Questions and Problems

Index

Douglas A. Skoog (deceased) was a professor of chemistry at Stanford University and the lead author of several best-selling texts during his career. He earned a B.S. in chemistry from Oregon State University and his Ph.D. in analytical chemistry from the University of Illinois. Dr. Skoog was the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. The same year, he was named a fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching.

Donald M. West (deceased) was a professor of chemistry at San Jose State University.

F. James Holler is professor emeritus of chemistry and is a recipient of the Alumni Association Great Teacher Award at the University of Kentucky. He received his Ph.D. from Michigan State University. In addition to his role as co-author of several bestselling texts, he is co-creator of the world-famous Periodic Table of Comic Books.

Stanley R. Crouch is professor emeritus at Michigan State University. He received his undergraduate and M.S. degrees from Stanford University and his Ph.D. in analytical chemistry from the University of Illinois. He is the recipient of the 2001 American Chemical Society Division of Analytical Chemistry Award in Chemical Instrumentation and the 1996 ACS Division of Analytical Chemistry Award for Excellence in Teaching.

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